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Iowa Department of Natural Resources_Airport Wastewater Treatment FacilityMasterpiece on the Mississippi TO: The Honorable Mayor and City Council Members FROM: Michael C. Van Milligen, City Manager SUBJECT: Dubuque Regional Airport Inspection Report DATE: June 17, 2010 Water Pollution Control Plant Manager Jonathan Brown has supplied information related to the June 11, 2010 letter from the Iowa Department of Natural Resources on the Dubuque Regional Airport Wastewater Treatment Facility Inspection. Michael C. Van Milligen MCVM:jh Attachment cc: Barry Lindahl, City Attorney Cindy Steinhauser, Assistant City Manager Jonathan R. Brown, Water Pollution Control Plant Manager Dubuque kritri All- AmedcaCiry 2007 Masterpiece on the Mississippi Michael C. Van Milligen, City Manager TO: FROM: Jonathan R. Brown, WPCP Manager SUBJECT: Dubuque Regional Airport Inspection Report DATE: June 17, 2010 INTRODUCTION BACKGROUND DISCUSSION Dubuque AY- Amerlca City y 2007 The purpose of this memo is to provide information concerning the recent inspection by IDNR of the Dubuque Regional Airport Wastewater Lagoon and to outline tasks that will be completed to fulfill the requirements and recommendations given as a result of the inspection report. On May 11, 2010 a routine inspection of the Dubuque Regional Airport Wastewater Treatment Lagoon was conducted by staff of the Iowa Department of Natural Resources and an inspection report was sent June 11, 2010. The Airport Lagoon is jointly operated by staff of the Airport and Water Pollution Control Department. The WPCP staff is responsible for monthly monitoring, reporting to IDNR, and major maintenance of mechanical equipment. Airport staff has taken responsibility for daily flow monitoring, weekly settleable solids testing, and general maintenance. The summary of requirements is listed below along with what action will be taken to fulfill these requirements; 1. Settleable solids testing must be conducted weekly and reported on the monthly operating report — This requirement fell through the cracks the last few months and will be reinitiated by WPCP and Airport staff. 2. Fecal coliform samples must be reported in units of 10 *3/100 ml. — This was caused by a misreading of the reporting form. All of the other reporting we do for fecal coliform is reported as colonies per 100 ml rather than in units of 1000 colonies per 100 ml. This error has been corrected with the report for the month of May. 3. The owner must initiate a program to identify and eliminate sources of I /1— WPCP staff and Airport staff will meet within two weeks to develop a plan to begin this study. 4. Algaecide must not be used — As indicated in the body of the report we have not used algaecide at this facility since 2004. 5. All valves and control equipment should be repaired and maintained in proper working order at all times and regularly exercised to keep valves in good working order. — As indicated in the report the mechanical equipment at the facility was in good working order. The suggestion given is what is currently being accomplished on a regular basis. We will review our maintenance record keeping making sure we are receiving credit for the work that is being done, 6. Within 30 days of the receipt of this report lift station pumps must be calibrated — The project will be completed prior to July 2, 2010 and a schedule adopted for yearly calibration. 7. If the operator determines that sludge must be removed from the lagoon, any sludge removed must be handled in accordance with 567 IAC Chapter 67. — We will complete the measurement of the sludge levels in the lagoons by August 1, 2010 and if needed removal will be done in compliance with the code. The recommendations given in the report will be incorporated in the routine operation of the facility. Airport and WPCP staff will coordinate discussion with IDNR staff to try and determine what the bacterial requirements will be for future NPDES permits. SUMMARY In general the operation of the Dubuque Regional Airport Lagoon with cooperation between Airport and WPCP staff has worked quite well and the plant is well maintained. WPCP and Airport staff will work together over the next few weeks to properly respond to the issues raised in the inspection report. ACTION REQUESTED The purpose of this memo is to report actions that will be taken to respond to the inspection report. Attachments: cc: Todd Dalsing Assistant Manager Dubuque Regional Airport Fields of Opportunities CHESTER J. CULVER, GOVERNOR PATTY JUDGE, LT. GOVERNOR June 11,2010 City of Dubuque City Hall 13th & Central Dubuque, IA 52001 ATTN: Honorable Mayor & City Council RE: Dubuque Regional Airport Wastewater Treatment Facility Inspection NPDES Permit #: 3126002 Dear Honorable Mayor & City Council: Enclosed is the report of the recent inspection of the above facility conducted by Sue Miller of the Field Office #1 staff. We believe you will find the report self - explanatory. All requirements listed in this report must be completed as identified in this report. If you have any questions about the inspection or report, please contact Sue Miller or myself at this office. Sincerely, Mike Wade Environmental Specialist FIELD OFFICE #1 / 909 West Main Suite 4 / Manchester, IA 52057 563 - 927 -2640 / FAX 563 - 927 -2075 / www.iowadnr.com STATE OF IOWA DEPARTMENT OF NATURAL RESOURCES RICHARD A. LEOPOLD, DIRECTOR cc: DNR Records Center, (w /encl.) Jonathon Brown, Dubuque Water Pollution Control Facility, 795 Julien Dubuque Dr., Dubuque, IA 52003 (w /encl.) File: Dubuque Regional Airport WW eFile: 31 WW Dubuque Regional Airport 051110 ins sjm c t3 • m • 0 • r o 0 no NPDES PERMIT COMPLIANCE SUMMARY SELF- MONITORING Operation Reports Submitted: PLANT GRADE: WW1 L Required Data on Reports: ❑ Unsat.* Testing Adequacy: ❑ Sat. ❑ Marg.* ❑ Unsat.* ►5 Sat. ❑ Marg.* ❑ Unsat.* ❑ Sat. ►4 Marg.* EFFLUENT LIMITATIONS SELF - MONITORING RESULTS: ❑ Unsatisfactory* ❑ Satisfactory ►1 Marginal* SAMPLES THIS INSPECTION TYPE: None LAB DATA ATTACHED? ❑Yes ❑ No RESULTS: ❑ Unsatisfactory* ❑ Satisfactory ►.1 Marginal* VISUAL APPEARANCE OF EFFLUENT: Tinted blue from algaecide VISUAL APPEARANCE OF RECEIVING STREAM: Effluent appears to soak into the ground. COMPLIANCE SCHEDULE COMPLIANCE w /SCHEDULE: ❑ Sat. ❑ Marg.* ❑ Unsat.* NEXT ITEM DUE: DATE DUE: FACILITY INFORMATION FACILITY NAME: Dubuque Regional Airport Wastewater Treatment Lagoon PLANT GRADE: WW1 L ADDRESS: RR #3 CITY: Dubuque STATE: Iowa ZIP: 52001 PHONE: 563- 589 -4176 PE (BOD): NA RESPONSIBLE AUTHORITY /OWNER: City of Dubuque RESPONSIBLE OPERATOR NAME: Jonathon Brown GRADE: IV CERTIFICATION NUMBER: DESIGN CAPACITY AVERAGE MGD: 0.006 MAXIMUM MGD: 0.006 POUNDS BOD /DAY: 5 PE (BOD): 30 NOW TREATING AVERAGE MGD: 0.005 MAXIMUM MGD: 0.009 POUNDS CBOD /DAY: NA PE (BOD): NA PERIOD REVIEWED: 01/01/01 — 03/31/04 POPULATION SERVED: Transient pop. RECEIVING STREAM Unnamed Tributary to Granger Creek B(LR) AUTHENTICATION INSPECTOR: NAME: ue Miller, Environmental Specialist �, 1 (1 DATE: C; / // / /Gs REVIEWER: " NAME: Mike Wade, 1( \L1 vironmental Specialist - DATE: 6,10-it INSPECTION INFORMATION INSPECTION DATE THIS INSPECTION: 05/11/2010 DATE LAST INSPECTION: 04/21/04 PURPOSE: Routine Compliance Inspection PERSONS INTERVIEWED NAME: Jonathon Brown (via telephone) Todd Dalsing TITLE: Wastewater Operator Acting Airport Manager NPDES Permit #: 3126002 IOWA DEPARTMENT OF NATURAL RESOURCES WASTEWATER TREATMENT FACILITY INSPECTION Page 1 of 4 GENERAL DESCRIPTION: Three cell, completely mixed aerated lagoon * Ex in Comments and Recommendations Section Parameter Sample Results Permit Maximum CBOD 18 mg /L 40 mg /L BOD 22 mg /L NA Total suspended Solids (TSS) 130 mg /L 120 mg /L pH 9.1 s.u. 6 -9 s.u. Ammonia Nitrogen (NH -N) 1.6 mg /L NA e. coli 28000 MPN /100 ml NA Parameter Sample Results CBOD 58 mg /L BOD 70 mg /L Total suspended Solids (TSS) 95 mg /L pH 8.4 s.u. Ammonia Nitrogen (NH -N) 38 mg /L Dubuque Regional Airport Wastewater Treatment Lagoon Inspection Inspection Date: 05/11/10 NPDES Permit #: 3126002 Page 2 NPDES PERMIT COMPLIANCE: The monthly operation reports (MORs) were reviewed for the reporting period from May 1, 2007 through April 30, 2010. Self- Monitoring — The operation reports were submitted regularly and on time; and it appears that the wastewater testing parameters of the NPDES permit are being consistently entered at the required frequencies on the monthly reports, except that settleable solids results are not being reported as required to be performed on the effluent weekly by the facility permit. In addition, fecal coliform samples must be reported in units of 10 ml. Design Capacity /Effluent Limitations — During the above mentioned reporting period the following observations were made: • The design influent flow rates are 0.006 MGD AWW and 0.006 MGD MWW. The AWW was exceeded during March 2010 and the MWW was exceeded eight (8) months during the reporting period. • The 30 -day and 7 -day average CBOD effluent limitations are 25 mg /L and 40 mg /L respectively. During the above mentioned reporting period the facility the 30 -day average was exceeded in September 2009 and April 2010. • The 30 -day and 7 -day average total suspended solids (TSS) effluent limitations are 80 mg /L and 120 mg /L respectively. During the above mentioned reporting period the facility the 30 -day average and 7 -day average were both exceeded in April 2010. Samples This Inspection — A 24 -hour composite influent sample and a grab sample of the final effluent were collected and submitted to the University Hygienic Laboratory (UHL) in Des Moines for analysis. The below list and attached copy of the test results indicates the sample results obtained and compliance with the effluent limitations of the current operation permit. 24 -hour composite influent sample results Grab effluent sample results Grab samples were also collected from both influent and effluent, which were analyzed for oil and grease. The influent sample contained 12.6 mg /L and the effluent sample was below detection. The airport should be aware of the activities that may be contributing oil and grease to the system and should develop strategies to prevent entry to the collection system. Dubuque Regional Airport Wastewater Treatment Lagoon Inspection Inspection Date: 05/11/10 NPDES Permit #: 3126002 Page 3 Total suspended solids in the effluent sample exceeded the 7 -day average permit limitation. The effluent sample TSS concentration was also higher than the influent TSS concentration. Algae forming in the lagoon cells is most likely responsible for this, however excess sludge buildup could also be a contributing factor. Analysis from samples collected for this inspection indicate that this facility is not meeting the 85% removal permit limits for CBOD5. A one day sample event is not adequate to evaluate this permit limit, but it does indicate that there may be a concern that adequate secondary treatment may not being provided at all times. FACILITY EVALUATION: Collection System — If the flow values are accurate, infiltration /inflow (1 /1) may be a contributing to the frequent maximum flow exceedances. Large amounts of clear water could be part of the cause of hydraulic overload reducing the efficiency of treatment units. These sources include, but are not limited to roof drains, basement sumps, storm sewer interconnections and leaking manholes. The owner must initiate a program to identify and eliminate sources of I /1. Lift Station(s) —The Dubuque Regional Airport is served by one lift station located across the road from the main terminal. The lift station appeared to be well maintained and clean. Aeration System — The aeration system consists of two submerged diffusers in each of cells 1 and 2. Cell 3 is a quiescent cell. Mr. Dalsing reported that the diffuser plates had recently been replaced. Lagoon Structures — The operator said that cell 3 has a problem with excess algae and duckweed growth. To control the excess growth; the maintenance crew had added an algaecide on a regular basis. The owner was required to stop using the algaecide as a result of the 2004 inspection. Aerated lagoons that have an abundance of blue -green algae present may be either organically overloaded or have some deficiency in the aeration system. Algaecide must not be used due to possible toxicity to aquatic life, unless effluent monitoring and limits are established by the NPDES permit. Mr. Brown reported that algaecides are not used. We recommend the mechanical or manual removal of floating algae mats. A layer of duckweed will also inhibit algae growth by shading the sunlight. Manual removal of the duckweed prior to cold weather will keep the dying duckweed from adding to the BOD of the cell. All valves and control equipment should be repaired and maintained in proper working order at all times and regularly exercised to keep the valves in good working order. Flow Measurement — Time clocks on the lift station pumps are used for calculating influent flow. This method of flow needs to be recalibrated at least every twelve months to take into account for impeller wear. According to Mr. Brown, the lift station pumps have not been calibrated since 2004. These calibrations must be kept with other maintenance records. As stated in the Collection System Section of this report, the reported influent flow readings for this system indicate that the system is hydraulically overloaded. Within 30 days of the receipt of this report, the operator must calibrate the lift station pumps to ensure that accurate flow data is provided to the department. The facility permit also requires instantaneous effluent flows. The outfall is not equipped with a flow measurement device. Dubuque Regional Airport Wastewater Treatment Lagoon Inspection Inspection Date: 05/11/10 NPDES Permit #: 3126002 Page 4 General Staffing — The operator of this facility is Jonathon Brown, who is also the operator of the City of Dubuque Water Pollution Control Facility. Airport personnel assist Mr. Brown with daily operations. Miscellaneous — A Use Assessment and Attainability Analysis was completed for the drainage ditch, the unnamed tributary and Granger Creek. No recreational designation was the recommended designation for the drainage ditch and the upper and middle reaches of the unnamed tributary (above the Highway 61 crossing.) Secondary Contact (2) recreational use was the recommended designation for the lower reach of the unnamed tributary and for Granger Creek. This recommendation, if approved, could result in e. coli limits in future NPDES permits for the Dubuque Regional Airport's wastewater lagoons. The Airport can request a "best guess" waste load allocation to determine potential effluent limitations based on the recommended designations. The e. coli results from the sample collected for this inspection indicate that the lagoons may have difficulty meeting bacteria limitations without disinfection. Sludge— The operator should investigate the thickness of the sludge layer in the lagoon cells. Too much sludge can limit the amount of available storage and could contribute to effluent totals suspended solids. If the operator determines that sludge must be removed from the lagoon, any sludge removed must be handled in accordance with 567 IAC Chapter 67. SUMMARY OF REQUIREMENTS 1. Settleable solids tests must be conducted weekly and reported on the monthly operating report. 2. Fecal coliform samples must be reported in units of 10 /100 ml. 3. The owner must initiate a program to identify and eliminate sources of 1 /1. 4. Algaecide must not be used due to possible toxicity to aquatic life, unless effluent monitoring and limits are established by the NPDES permit. 5. All valves and control equipment should be repaired and maintained in proper working order at all times and regularly exercised to keep the valves in good working order. 6. Within 30 days of the receipt of this report, the operator must calibrate the lift station pumps to ensure that accurate flow data is provided to the department. 7. If the operator determines that sludge must be removed from the lagoon, any sludge removed must be handled in accordance with 567 IAC Chapter 67. SUMMARY OF RECOMMENDATIONS 1. We recommend the mechanical or manual removal of floating algae mats. A layer of duckweed will also inhibit algae growth by shading the sunlight. Manual removal of the duckweed prior to cold weather will keep the dying duckweed from adding to the BOD of the cell. 2. The Airport can request a "best guess" waste load allocation to determine potential effluent limitations based on the recommended designations. The e. coli results from the sample collected for this inspection indicate that the lagoons may have difficulty meeting bacteria limitations without disinfection. 3. The operator should investigate the thickness of the sludge layer in the lagoon cells. Too much sludge can limit the amount of available storage and could contribute to effluent totals suspended solids. 1 THE UNIVERSITY OF IOWA May 26, 2010 Sue Miller EPD 1 909 West Main Suite 4 Manchester, IA 52057 Sue, Enclosed are the "Results of Analyses" for the compliance sampling inspection at the Dubuque Regional airport sampled on May 11 -12, 2010. If you have any questions regarding the results, or any other questions, please contact Mike Schueller or myself. Sincerely, -fie .Q Todd Hubbard HYGIENIC LABORATORY Iowa's Environmental and Public Health Laboratory 102 Oakdale Campus, H101 OH Iowa City, Iowa 52242 -5002 319 - 335 -4500 Fax 319 - 335 -4555 www.uhl.uiowa.edu Analyte Concentration gpd Quantitation Limit gpd Flow Rate 4541 0.001 HYGIENIC LABORATORY The University of Iow• Comments Date Analyzed: 05 -13 -2010 Method: SM 5210B Date Analyzed: 05 -12 -2010 Method: ISCO,1989 Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors MASON CITY IA 50401 -5630 Hygienic Laboratory The University of Iowa Date of report: 05 -26 -2010 I IIIIIIIIIIIIIIIII IIIIIIIIIIIIIIIIIIIIIIIIIIII SUE MILLER IDNR -FO 2 2300 15TH STREET SW Upon arrival, sample met container and preservation requirements for the analysis requested. Please review carefully your sample results for additional analyte comments or method exceptions. Influent sampled from lift station. 5/11- 12/10. 1025 -1005 Samples collected every 20 minutes, all samples collected. Date Analyzed: 05 -18 -2010 Analyzed at: Ankeny Method: EPA MCD -51 Analyte Total Biochemical Oxygen Demand (5 day) Carbonaceous BOD (5 day) Comments Concentration mg /L 70 58 Quantitation Limit mg /L 2 Reported result was based on a dilution that did not meet SM criteria for at least 2.0 mg/L DO depletion. The result does not meet all criteria for NPDES data validity and must be qualified as an estimate if reported to IDNR for discharge permit purposes. Based on the measured DO depletion for the dilution containing the greatest volume of sample the calculated BOD(C) is 58 mg/L. 2 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Results of Analyses Sampling Comments Biochemical Oxygen Demand Analyzed at: Iowa City Flow Rate for Compliance Activities Analyzed at: Ankeny Page 1 - Continued on next page Sample Number Date Received Project Date Collected Collection Site Collection Town Description Reference Collector Phone Purchase Order htip://www.uhLuiowa.edu 2010015475 05 -12 -2010 03WQCSI 05 -12 -2010 10:05 airport infl 24hr composite Dubuque waste water HUBBARD UHL0004 u __, ? a' C J E MAY 27 2010 DNR F.0.1 Analyst: CTH Verified: KS Analyst: RAD Verified: DM Analyst: CTH Verified: KS Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 Analyte Concentration mg /L Quantitation Limit mg /L Ammonia Nitrogen as N 38 0.05 HYGIENIC LABORATORY The University of Iowa Analyte Total Suspended Solids Comments Concentration mg /L 95 Quantitati mg /L 1 Dried at 103 degrees C Date Analyzed: 05 -14 -2010 Method: USGS I- 3765 -85 Date Analyzed: 05 -19 -2010 Method: LAC10- 107 -06 -1J Michael D. Wickman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors mg /L - Milligrams per Liter gpd - Gallons per Day Hygienic Laboratory The University of Iowa 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Total Suspended Solids Analyzed at: Ankeny Ammonia as N Analyzed at: Ankeny Iowa Environmental Laboratory IDs are: Ankeny #397, Iowa City #027, Lakeside #393. If you have any questions please call Client Services at 800 /421 -IOWA (4692) or 319/335 -4500. Thank you. Page 2 - End of Report http://www.uhl.utowa.edu Page 2 Sample Number 2010015475 Analyst: MP Verified: LF on Limit Analyst: JE Verified: LF Description of units used within this report No Units - No Units Quant Limit - Lowest concentration reliably measured The results of this report relate only to the items analyzed. This report shall not be reproduced except in full without the written approval of the laboratory. Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 Analyte Concentration mg /L Quantitation Limit mg /L Hexane Extractable Material (HEM) <5.00 5.00 HYGIENIC LABORATORY The University of Iowa 6 1.1.1.IIfffuIfuIII IIIIIIIIII....11IIIIffuIIIII SUE MILLER IDNR -FO 2 2300 15TH STREET SW MASON CITY IA 50401 -5630 Comments Date of report: 05 -26 -2010 Sample Number Date Received Project Date Collected Collection Site Collection Town Description Reference Collector Phone Purchase Order 2010015476 05 -12 -2010 03WQCSI 05 -12 -2010 09: airport effluent Dubuque waste water HUBBARD UH Upon arrival, sample met container and preservation requirements for the analysis requested. Please review carefully your sample results for additional analyte comments or method exceptions. Sampling Comments Grab sample collected at last discharge point from polishing pond. 5/12/10. 0915. Date Analyzed: 05 -18 -2010 Method: EPA MCD -51 Date Analyzed: 05 -13 -2010 Method: SM 5210B Date Analyzed: 05 -24 -2010 Method: EPA 1664 Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors Hygienic Laboratory The University of Iowa 102 Oakdale Campus, #101 011 Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Results of Analyses Analyzed at: Ankeny Biochemical Oxygen Demand Analyzed at: Iowa City Oil & Grease (Reported as HE Analyzed at: Iowa City Page 1 - Continued on next page http: //www.uhl. uiowa. edu Analyst: KB Verified: GJ 15 frab L0004 Analyst: CTH Verified: KS Analyte Total Biochemical Oxygen Demand (5 day) Carbonaceous BOD (5 d a ) Comments Concentration mg /L 22 18 Results should be qualified for Total BOD only (CBOD results do not require a qualifier): Reported result was based on a dilution criteria for at least 1.0 mg/L remaining DO. The Result does not meet all criteria for NPDES data validity and must be qualified a an estimate if reported to IDNR for discharge permit purposes. Depletion of the dilution containing the least amount of sample was such that no valid estimate of BOD is possible. The true result is possibly much greater than the reported value. Quantitation Limit mg /L 2 2 Analyst: RAD Verified: DM Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 Analyte Concentration mg /L Quantitation Limit mg /L Ammonia Nitrogen as N 1.6 0.05 Analyte Concentration Degrees C Quantitation Limit Degrees C Field Temperature 10.7 0.0 Analyte Concentration pH Units Quantitation Limit pH Units Field pH 9.1 10 Analyte Concentration MPN /100mL Quantitation Limit MPN/ 100mL E.coli 28000 10 HYGIENIC LABORATORY The Uei•errity of Iowa The University of Iowa Hygienic Laboratory Date Analyzed: 05 -12 -2010 Method: SM 18 9223 Date Analyzed: 05 -12 -2010 Method: SM 4500 H E.coli MPN by Method 9223B Analyzed at: Iowa City Field nH Analyzed at Ankeny Field Temperature Page 2 Sample Number 2010015476 Analyst: CL /M Verified: KO Analyst: CTH Verified: KS Date Analyzed: 05 -12 -2010 Method: SM 2550 Analyte Total Suspended Solids Comments Concentration mg /L 130 Quantitation Limit mg /L Dried at 103 degrees C 1 Date Analyzed: 05 -14 -2010 Method: USGS I- 3765 -85 Date Analyzed: 05 -19 -2010 Method: LAC10- 107 -06 -1J Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Analyzed at: Ankeny Total Suspended Solids Analyzed at: Ankeny Ammonia as N Analyzed at: Ankeny Page 2 - Continued on next page http: / /www. uhl. uiowa. edu Analyst: CTH Verified: KS Analyst: MP Verified: LF Analyst: JE Verified: LF Description of units used within this report mg /L - Milligrams per Liter pH Units - pH Units Degrees C - Degrees Celsius No Units - No Units MPN /100mL - Most Probable Number per 100 Milliliters Quant Limit - Lowest concentration reliably measured The results of this report relate only to the items analyzed. This report shall not be reproduced except in full without the written approval of the laboratory. Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 HYGIENIC LABORATORY The University of Ioas Hygienic Laboratory The University of Iowa Iowa Environmental Laboratory IDs are: Ankeny #397, Iowa City #027, Lakeside #393. If you have any questions please call Client Services at 800/421 -IOWA (4692) or 319/335 -4500. Thank you. Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Page 3 - End of Report http://www.uhLuiowa.edu Page 3 Sample Number 2010015476 Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 Analyte Concentration Degrees C Quantitation Limit Degrees C Field Temperature 11.8 0.0 Analyte Concentration pH Units Quantitation Limit pH Units Field pH 8.4 5.00 Analyte Concentration mg/L Quantitation Limit mg /L Hexane Extractable Material (HEM) 12.6 5.00 HYGIENIC LABORATORY The University of Iowa Comments Date of report: 05 -26 -2010 I,I,I,II,t „1„111 IIIIIII,IIJIIIIIIIIuIIIIII�I SUE MILLER IDNR -FO 2 2300 15TH STREET SW MASON CITY IA 50401 -5630 Sample Number Date Received Project Date Collected Collection Site Collection Town Description Reference Collector Phone Purchase Order 2010015477 05 -12 -2010 03WQCSI 05 -12 -2010 09: airport influent Dubuque waste water HUBBARD UH Upon arrival, sample met container and preservation requirements for the analysis requested. Please review carefully your sample results for additional analyte comments or method exceptions. ate Analyzed: 05 -24 -2010 Method: EPA 1664 ate Analyzed: 05 -12 -201 Method: SM 4500 H ate anatyzea: uo -11- Method: SM 2550 mg /L - Milligrams per Liter Degrees C - Degrees Celsius Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors Hygienic Laboratory The University of Iowa 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Results of Analyses Oil & Grease (Reported as HE Analyzed at: Iowa City Field nH Analyzed at Ankeny Field Tem p ratur Analyzed at: Ankeny Iowa Environmental Laboratory IDs are Ankeny #397, Iowa City #027, Lakeside #393. Page 1 - Continued on next page http:/lwww.uhl.uiowa.edu Analyst: KB Verified: GJ 25 grab Analyst: CTH Verified: KS Analyst: CTH Verified: KS L0004 Description of units used within this report pH Units - pH Units Quant Limit - Lowest concentration reliably measured The results of this report relate only to the items analyzed. This report shall not be reproduced except in full without the written approval of the laboratory. Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642 HYGIENIC LABORATORY The University of Ins. Hygienic Laboratory The University of Iowa If you have any questions please call Client Services at 800/421 -IOWA (4692) or 319/335 -4500. Thank you. Michael D. Wichman, Ph.D. Michael A. Pentella, Ph.D. Associate Directors 102 Oakdale Campus, #101 OH Iowa City, Iowa 52242 -5002 319/335 -4500 Fax: 319/335 -4555 Page 2 - End of Report http://www.uhLuiowa.edu Page 2 Sample Number 2010015477 Iowa Laboratories Complex 2220 S. Ankeny Blvd, Ankeny, Iowa 50023 515/725 -1600 Fax: 515/725 -1642